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Disinfection Theory & Chemistry · 7 min read

Free vs. Combined vs. Total Chlorine: The DPD Test Explained

What HOCl and OCl− actually do, why pH changes their ratio, and how to read a DPD test block correctly.

Most test strips and kits report three numbers: free chlorine (FC), combined chlorine (CC), and total chlorine (TC = FC + CC). Each one tells you something different about the pool's sanitation.

The two active forms of chlorine

When you add chlorine to water, it splits into two forms depending on pH:

  • HOCl (hypochlorous acid): the active, strong form. Kills pathogens quickly.
  • OCl⁻ (hypochlorite ion): a much weaker form. Much slower to disinfect.

Both count as “free chlorine” on the test — but their kill-power differs by ~100×.

The pH/HOCl table (memorize this)

pH% HOCl (active)% OCl⁻ (weak)
6.5~90%~10%
7.0~75%~25%
7.4~57%~43%
7.5~50%~50%
7.8~33%~67%
8.0~22%~78%

This is why a pool with 3 ppm FC at pH 8.0 sanitizes worse than a pool with 2 ppm FC at pH 7.4. Same chlorine level — very different effectiveness.

Combined chlorine: what it actually is

When free chlorine bonds with ammonia (from urine, sweat, organic matter), it forms chloramines:

  • Monochloramine (NH₂Cl): relatively stable, modest irritant
  • Dichloramine (NHCl₂): stronger smell, strong irritant
  • Trichloramine (NCl₃): the “chlorine smell” in public pools and the main respiratory irritant

All three register as combined chlorine on a DPD test. The “chlorine smell” people blame on “too much chlorine” is actually too little chlorine— there's not enough free chlorine to destroy the chloramines.

How to read a DPD test correctly

A standard DPD test block:

  1. Fill the sample vial to the line with pool water (from elbow depth, away from returns).
  2. Add DPD Reagent 1 drops. Cap and invert. Read color — this is free chlorine (FC).
  3. Add DPD Reagent 3 drops to the same sample. Cap and invert. Read new color — this is total chlorine (TC).
  4. Combined chlorine = TC − FC.

For precision, use FAS-DPD titration (e.g., Taylor K-2006) — reads to 0.2 ppm instead of 0.5 ppm color-block resolution.

Target numbers

  • FC: 1–3 ppm (residential, unstabilized) / 3–5 ppm typical with CYA 30–50 ppm
  • CC: < 0.2 ppm
  • If CC is > 0.5 ppm: shock to breakpoint (10×CC)

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